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<meta http-equiv="Content-Type" content="text/html; charset=Windows-1252"></head><body style="word-wrap: break-word; -webkit-nbsp-mode: space; -webkit-line-break: after-white-space; color: rgb(0, 0, 0); font-size: 14px; font-family: Calibri, sans-serif; "><div><br></div><span id="OLK_SRC_BODY_SECTION"><div><div lang="EN-US" link="blue" vlink="purple"><div class="WordSection1"><p class="MsoNormal"><o:p> </o:p></p><p class="MsoNormal" align="center" style="mso-margin-top-alt:auto;mso-margin-bottom-alt:auto;text-align:center;line-height:150%;background:white"><b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">MS DEFENSE STUDENT: </span></b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">Anh Vu</span><span style="font-size:11.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"><o:p></o:p></span></p><p class="MsoNormal" align="center" style="mso-margin-top-alt:auto;mso-margin-bottom-alt:auto;text-align:center;line-height:150%;background:white"><b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">DATE: </span></b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">Friday, April 21, 2017</span><span style="font-size:11.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"><o:p></o:p></span></p><p class="MsoNormal" align="center" style="mso-margin-top-alt:auto;mso-margin-bottom-alt:auto;text-align:center;line-height:150%;background:white"><b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">TIME: </span></b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">2:30 PM</span><span style="font-size:11.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"><o:p></o:p></span></p><p class="MsoNormal" align="center" style="mso-margin-top-alt:auto;mso-margin-bottom-alt:auto;text-align:center;line-height:150%;background:white"><b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">PLACE:</span></b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"> Room E132 (Engineering Building
2)</span><span style="font-size:11.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"><o:p></o:p></span></p><p class="MsoNormal" align="center" style="mso-margin-top-alt:auto;margin-bottom:8.0pt;text-align:center;line-height:150%;background:white"><b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">DISSERTATION CHAIR:
</span></b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">Dr. Lars Grabow
</span><span style="font-size:11.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"><o:p></o:p></span></p><div style="margin-bottom:8.0pt"><div class="MsoNormal" align="center" style="margin-bottom:0in;margin-bottom:.0001pt;text-align:center;line-height:150%;background:white"><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"><hr size="2" width="100%" align="center"></span></div></div><p class="MsoNormal" align="center" style="mso-margin-top-alt:auto;mso-margin-bottom-alt:auto;text-align:center;line-height:150%;background:white"><b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO">TITLE:<o:p></o:p></span></b></p><p class="MsoNormal" align="center" style="mso-margin-top-alt:auto;mso-margin-bottom-alt:auto;text-align:center;line-height:150%;background:white"><b><span style="font-size:14.0pt;line-height:150%;color:black">NOx Storage and Release Activity on Pd/BEA Passive NOx Adsorber</span></b><b><span style="font-size:14.0pt;line-height:150%;color:black;letter-spacing:0pt;mso-fareast-language:KO"><o:p></o:p></span></b></p><p class="MsoNormal" style="mso-margin-top-alt:auto;margin-bottom:0in;margin-bottom:.0001pt;text-align:justify;text-indent:.5in"><span style="color:windowtext">Increasingly stringent vehicular emission regulation on NO<sub>x</sub> demands a better strategy to further mitigate tailpipe NO<sub>x</sub> exhaust. In terms of NO<sub>x</sub> reduction strategy, both current state-of-the-art
technologies, selective catalytic reduction (SCR) and NO<sub>x</sub> storage and reduction (NSR), have shown optimal performance in warm conditions but are not fully functional at temperature below 200°C, commonly regarded cold-start condition. Thus, in order
to lower NOx cold-start emission, the passive NO<sub>x</sub> adsorber (PNA) has been introduced based on the concept of low-temperature NO<sub>x</sub> storage developed during the research of NSR, with so far a very promising result thanks in part to high
through-put comprehensive catalyst screening. Among the PNAs, Pd/BEA stands out due to its promising NO<sub>x</sub> storage capacity and well-controlled thermal desorption performance. In this Masters thesis, the NO<sub>x</sub> activity on Pd/BEA passive NO<sub>x</sub>
adsorber was investigated.<o:p></o:p></span></p><p class="MsoNormal" style="mso-margin-top-alt:auto;margin-bottom:0in;margin-bottom:.0001pt;text-align:justify;text-indent:.5in"><span style="color:windowtext">NO<sub>x</sub> adsorption and desorption on Pd/BEA was studied using temperature-programmed desorption method. It was shown that CO improved NO<sub>x</sub> storage and induced NO<sub>x</sub> release to higher temperature on Pd/BEA.
In-situ diffuse reflectance IR spectroscopy revealed the critical role of Pd chemical states, where lower oxidation state Pd would bind NO<sub>x</sub> more strongly. In addition to CO, the influence of SO<sub>2</sub> was also addressed briefly and was shown
to slightly decrease NO<sub>x</sub> performance on Pd/BEA, especially when CO was included in the feed.<o:p></o:p></span></p><p class="MsoNormal" style="mso-margin-top-alt:auto;margin-bottom:0in;margin-bottom:.0001pt;text-align:justify"><span style="color:windowtext">Apart from the effect of gases, the desorption kinetics of NO<sub>x</sub> on Pd/BEA was also studied in an attempt to resolve the effect of heating rate on the controlled release of NO<sub>x</sub>. As the ideal PNA demands surface
NOx to be retained until approximately 200°C before its desorption for downstream reduction (by SCR or NSR, which reaches maximum performance by that temperature), the heating rate becomes critical. Thermal desorption spectra were collected at different heating
rate and were subsequently analyzed using a number of methods, including the well-known Polanyi-Wigner model, Redhead’s method, and peak width analysis. The kinetic set of activation energy of desorption,
</span><!--[if gte msEquation 12]><m:oMath><m:sSub><m:sSubPr><span style='font-family:"Cambria Math","serif";font-style:italic'><m:ctrlPr></m:ctrlPr></span></m:sSubPr><m:e><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>E</m:r></span></i></m:e><m:sub><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>d</m:r></span></i></m:sub></m:sSub></m:oMath><![endif]--><!--[if !msEquation]--><span style="font-size: 12pt; line-height: 115%; font-family: 'Times New Roman', serif; color: rgb(51, 51, 51); position: relative; top: 5.5pt; letter-spacing: 0.1pt; "><img width="17" height="22" id="_x0000_i1025" src="cid:image002.png@01D2B781.6AD76190"></span><!--[endif]--><span style="color:windowtext">,
and frequency factor, </span><!--[if gte msEquation 12]><m:oMath><m:sSub><m:sSubPr><span style='font-family:"Cambria Math","serif";font-style:italic'><m:ctrlPr></m:ctrlPr></span></m:sSubPr><m:e><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>ν</m:r></span></i></m:e><m:sub><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>n</m:r></span></i></m:sub></m:sSub></m:oMath><![endif]--><!--[if !msEquation]--><span style="font-size: 12pt; line-height: 115%; font-family: 'Times New Roman', serif; color: rgb(51, 51, 51); position: relative; top: 5.5pt; letter-spacing: 0.1pt; "><img width="16" height="22" id="_x0000_i1025" src="cid:image003.png@01D2B781.6AD76190"></span><!--[endif]--><span style="color:windowtext">,
produced from the first two methods differed from that obtained from the last one. However, via a better fit in the full simulation of experimental TPD data, the latter desorption kinetics, computed from peak width analysis, became more reliable. The discrepancy
in (</span><!--[if gte msEquation 12]><m:oMath><m:sSub><m:sSubPr><span style='font-family:"Cambria Math","serif";font-style:italic'><m:ctrlPr></m:ctrlPr></span></m:sSubPr><m:e><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>E</m:r></span></i></m:e><m:sub><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>d</m:r></span></i></m:sub></m:sSub></m:oMath><![endif]--><!--[if !msEquation]--><span style="font-size: 12pt; line-height: 115%; font-family: 'Times New Roman', serif; color: rgb(51, 51, 51); position: relative; top: 5.5pt; letter-spacing: 0.1pt; "><img width="17" height="22" id="_x0000_i1025" src="cid:image002.png@01D2B781.6AD76190"></span><!--[endif]--><span style="color:windowtext">,
</span><!--[if gte msEquation 12]><m:oMath><m:sSub><m:sSubPr><span style='font-family:"Cambria Math","serif";font-style:italic'><m:ctrlPr></m:ctrlPr></span></m:sSubPr><m:e><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>ν</m:r></span></i></m:e><m:sub><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>n</m:r></span></i></m:sub></m:sSub></m:oMath><![endif]--><!--[if !msEquation]--><span style="font-size: 12pt; line-height: 115%; font-family: 'Times New Roman', serif; color: rgb(51, 51, 51); position: relative; top: 5.5pt; letter-spacing: 0.1pt; "><img width="16" height="22" id="_x0000_i1025" src="cid:image003.png@01D2B781.6AD76190"></span><!--[endif]--><span style="color:windowtext">)
obtained across the TPD data at different heating rate was reconciled by the compensation effect, which eventually established an empirical relationship between
</span><!--[if gte msEquation 12]><m:oMath><m:sSub><m:sSubPr><span style='font-family:"Cambria Math","serif";font-style:italic'><m:ctrlPr></m:ctrlPr></span></m:sSubPr><m:e><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>E</m:r></span></i></m:e><m:sub><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>d</m:r></span></i></m:sub></m:sSub></m:oMath><![endif]--><!--[if !msEquation]--><span style="font-size: 12pt; line-height: 115%; font-family: 'Times New Roman', serif; color: rgb(51, 51, 51); position: relative; top: 5.5pt; letter-spacing: 0.1pt; "><img width="17" height="22" id="_x0000_i1025" src="cid:image002.png@01D2B781.6AD76190"></span><!--[endif]--><span style="color:windowtext">
and </span><!--[if gte msEquation 12]><m:oMath><m:sSub><m:sSubPr><span style='font-family:"Cambria Math","serif";font-style:italic'><m:ctrlPr></m:ctrlPr></span></m:sSubPr><m:e><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>ν</m:r></span></i></m:e><m:sub><i><span style='font-family:"Cambria Math","serif";color:windowtext'><m:r>n</m:r></span></i></m:sub></m:sSub></m:oMath><![endif]--><!--[if !msEquation]--><span style="font-size: 12pt; line-height: 115%; font-family: 'Times New Roman', serif; color: rgb(51, 51, 51); position: relative; top: 5.5pt; letter-spacing: 0.1pt; "><img width="16" height="22" id="_x0000_i1025" src="cid:image003.png@01D2B781.6AD76190"></span><!--[endif]--><span style="color:windowtext">
and contributed to the predictability of the model developed from the peak-width analysis.</span><o:p></o:p></p></div></div></div></span><style><!--
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div.WordSection1
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ol
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ul
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--></style></body></html>