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<h2><span style="font-family:Tahoma">PhD Dissertation Announcement<o:p></o:p></span></h2>
<p class="MsoNormal"><b><span style="font-size:11.0pt;mso-bidi-font-size:10.0pt;
font-family:Tahoma"> </span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:14.0pt;font-family:Tahoma">Phase Behavior of
Polymer-Grafted Nanoparticles<o:p></o:p></span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:14.0pt;font-family:Tahoma"> </span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:14.0pt;font-family:Tahoma">Katrina Irene
Mongcopa<o:p></o:p></span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma"> </span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma">Date: July 24, 2015<o:p></o:p></span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma"> </span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma">Place: Chemical Engineering
Conference Room (S255)<o:p></o:p></span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma">Time: 10:30 AM<o:p></o:p></span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma"> </span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma">Committee Chair: </span></b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:Tahoma">Dr.
Ramanan Krishnamoorti<b><o:p></o:p></b></span></p>
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Tahoma"> </span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><b><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:
Tahoma">Committee Members:<o:p></o:p></span></b></p>
<p class="MsoNormal" align="center" style="text-align:center"><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:Tahoma">Dr.
Megan Robertson<o:p></o:p></span></p>
<p class="MsoNormal" align="center" style="text-align:center"><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:Tahoma">Dr.
Jacinta Conrad<o:p></o:p></span></p>
<p class="MsoNormal" align="center" style="text-align:center"><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:Tahoma">Dr.
Haleh Ardebili<o:p></o:p></span></p>
<p class="MsoNormal" align="center" style="text-align:center"><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:Tahoma">Dr.
Yandi Hu<o:p></o:p></span></p>
<p class="MsoNormal"><span style="font-size:12.0pt;font-family:Calibri;
mso-bidi-font-family:Tahoma"> </span></p>
<p class="MsoNormal"><span style="font-size:12.0pt;font-family:Calibri;
mso-bidi-font-family:Tahoma"> </span></p>
<p class="MsoNormal" style="text-align:justify;text-indent:.5in">The fundamental
thermodynamic interactions between polymer-grafted nanoparticles and their
surroundings—whether in a polymer matrix or a solvent—are crucial to the
properties and performance of the resulting material. The phase behavior and
conformations of the grafted polymer are governed by both entropic and
enthalpic effects that in turn, drive dispersion and aggregation in the system.
Although the dispersion-aggregation transition in the athermal case is largely
entropic in nature, significant enthalpic interactions exist in many chemically
dissimilar graft-matrix and graft-solvent systems that influence their phase
transition.<o:p></o:p></p>
<p class="MsoNormal" style="text-align:justify;text-indent:.5in"><o:p> </o:p></p>
<p class="MsoNormal" style="text-align:justify;text-indent:.5in">In this work,
the phase behavior and conformational transitions of polystyrene (PS)-grafted
silica nanoparticles in a poly(vinyl methyl ether) (PVME) matrix and
cyclohexane are investigated—both systems exhibit conformational changes in the
brush as a function of temperature. Through a combination of transmission
electron microscopy imaging, small angle x-ray and neutron scattering
techniques, a gradual wetting-dewetting transition in the silica-PS/PVME
composite is elucidated and found to be distinct from the
dispersion-aggregation transition. This is in stark contrast to athermal
systems of chemically similar brush and matrix chains where the two transition
events are analogous. Moreover, using light and neutron scattering, a
coil-to-globule transition of the grafted PS chains in cyclohexane is probed as
the solvent quality changes from good to poor. Measurements of the hydrodynamic
size reveal a continuous change from a highly-swollen brush to a globule-like
configuration before particle aggregation occurs. These observations are consistent
with changes in the brush thickness and radius of gyration measured from
neutron scattering experiments.<o:p></o:p></p>
<p class="MsoNormal" style="text-align:justify;text-indent:.5in"><span style="font-size:12.0pt;font-family:Calibri;mso-bidi-font-family:Tahoma"> </span></p>
<p class="MsoNormal" style="text-align:justify;text-indent:.5in">This work
presents key insights into the thermodynamic behavior of polymer-grafted
nanoparticles unique to dissimilar graft-matrix and graft-solvent systems.
Furthermore, it highlights fundamentally important concepts crucial to the
design and functionality of advanced materials.<o:p></o:p></p>
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panose-1:2 11 6 4 3 5 4 4 2 4;}
@font-face
{font-family:"Century Gothic";
panose-1:2 11 5 2 2 2 2 2 2 4;}
/* Style Definitions */
p.MsoNormal, li.MsoNormal, div.MsoNormal
{margin:0in;
margin-bottom:.0001pt;
font-size:12.0pt;
font-family:"Times New Roman","serif";}
a:link, span.MsoHyperlink
{mso-style-priority:99;
color:blue;
text-decoration:underline;}
a:visited, span.MsoHyperlinkFollowed
{mso-style-priority:99;
color:purple;
text-decoration:underline;}
p
{mso-style-priority:99;
mso-margin-top-alt:auto;
margin-right:0in;
mso-margin-bottom-alt:auto;
margin-left:0in;
font-size:12.0pt;
font-family:"Times New Roman","serif";}
p.MsoAcetate, li.MsoAcetate, div.MsoAcetate
{mso-style-priority:99;
mso-style-link:"Balloon Text Char";
margin:0in;
margin-bottom:.0001pt;
font-size:8.0pt;
font-family:"Tahoma","sans-serif";}
span.apple-tab-span
{mso-style-name:apple-tab-span;}
span.BalloonTextChar
{mso-style-name:"Balloon Text Char";
mso-style-priority:99;
mso-style-link:"Balloon Text";
font-family:"Tahoma","sans-serif";}
span.EmailStyle21
{mso-style-type:personal-reply;
font-family:"Calibri","sans-serif";
color:#1F497D;}
.MsoChpDefault
{mso-style-type:export-only;
font-size:10.0pt;}
@page WordSection1
{size:8.5in 11.0in;
margin:1.0in 1.0in 1.0in 1.0in;}
div.WordSection1
{page:WordSection1;}
--></style></body></html>